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不锈钢的电子轰击放气影响特性研究

Influence Study on the Characteristics of Electron Bombardment Induced Outgassing of Stainless Steel

  • 摘要: 电子轰击放气对一些真空系统的设计起到决定性作用,但电子轰击放气的影响因素很多。采用典型的真空腔室材料316L不锈钢,开展了电子轰击参数对放气的影响特性实验研究。结果表明,电子束首次轰击新鲜表面时,电子轰击放气响应是立即且剧烈的,后续轰击虽仍为即时响应,但强度显著衰减;随电子束累积剂量的增加,电子轰击放气量和电子产额逐渐下降,降至初始值的近一半;随电子通量的增加,电子轰击放气量和电子产额略微增加;随轰击电子能量的增加,电子轰击放气量和电子产额逐渐增加;电子束轰击表面积也会显著影响材料的放气响应,随着轰击面积增大,电子产额会迅速增至初始值的8倍。316L不锈钢的电子轰击放气组分主要是H2,此外还会释放出N2/CO和CO2,且这些放气组分的离子流也受电子束轰击参数的影响。

     

    Abstract: Electron bombardment induced outgassing plays a critical role in the design of specific vacuum systems, with numerous bombarding factors influencing its behavior. An investigation was undertaken to analyze the impacts of these electron bombarding factors using 316L stainless steel, a typical vacuum material. The findings demonstrate that initial outgassing is immediate and dramatic, while subsequent electron exposure results in an immediate but less dramatic outgassing response, highlighting the significant impact of the fresh surface on outgassing properties. Furthermore, as the electron dose increases, both the outgassing amount and electron yield gradually decrease to almost half of their original values. Conversely, increasing electron flux leads to a slight increase in electron yield. Additionally, increasing bombarding electron energy results in a gradual increase in outgassing amount or electron yield. Moreover, the bombarding area significantly influences electron induced outgassing; specifically, as the bombarding size increases, the electron yield rapidly increases to eight times its original value. The primary gas component released from 316L stainless steel during electron exposure is H2 along with some N2/CO and CO2; however, there is almost no outgassing of H2O or O2. Moreover, the ion current of these outgassed components detected by the residual gas analyzer (RGA) is also affected by parameters related to electron beam bombardment.

     

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