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电子致放气测试装置的研究

Electron Induced Outgassing Test Device

  • 摘要: 材料表面吸附的气体分子在电子轰击作用下,会加速释放到真空系统中。为了测试在电子轰击下的材料放气特性,研制了一套电子致放气的测试装置。电子束发生器作为重要的组成部件,具有许多可调参数,这些参数会在一定程度上影响输出的电子束质量,进而影响电子致放气测试结果。文章首先通过实验测量了电子束斑和束流的影响因素,结果表明,聚焦电压和栅极电压对束斑的尺寸有直接的影响,而能量电压对电子束斑直径没有影响。此外,阴极电压、电子能量和栅极电压都可影响到发射电流,从而影响出射的电子束电流。为了验证装置的电子致放气测试能力,采用放气率很低的316 L不锈钢作为测试样品,比较测试其经过三次电子束轰击前后的放气特性。结果表明,经过除气的316 L不锈钢的电子致放气率可较明显地测定,且电子束轰击下放气的主要成分由N2/CO变为H2

     

    Abstract: An electron induced outgassing test device was developed to measure the material outgassing properties under electron bombarding, and one of the most important units is the electron beam generator, which has many adjustable parameters that can affect the output beam quality. Experiments were carried out to measure the influence factors of electron beam spot and beam current. The results showed that both the focus voltage and grid voltage have a direct effect on the size of the electron beam spot. However, the energy voltage almost has no effect on the spot diameter. In addition, either cathode voltage, electron energy, or grid voltage can affect the emission current, and so as to the outgoing electron beam current, although the changing trend of the influence curve varies. In order to demonstrate the testing capability of the device for electron-stimulated desorption and outgassing, 316 L stainless steel with degassing treatment was selected as the test sample, and the outgassing characteristics before and after electron bombardment were tested and compared three times. It is indicated that the electron induced outgassing rate can be determined obviously for the sample. The main outgassing component under electron bombardment changes from N2/CO to H2.

     

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