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工作参数对电场增强高功率脉冲磁控溅射的调制作用研究

Influence of Deposition Conditions on Performance of Field Enhanced High Power Impulse Magnetron Sputtering Reactor

  • 摘要: 基于辅助阳极的电场增强高功率脉冲磁控溅射 (HiPIMS) 技术改善了常规HiPIMS放电及镀膜过程。研究工作参数对电场增强HiPIMS的调制作用可为该技术的应用提供理论依据。利用数字示波器收集HiPIMS基体离子电流, 分析了不同工作气压、靶基间距、脉冲频率和脉冲宽度等工作参数对基体离子电流的调制作用规律。利用扫描电镜观察了钒膜的截面形貌特征。结果表明:在相同的靶电压下, 基体离子电流平均值随工作气压的增加而增加并逐渐达到饱和值;随靶基间距的增加基体离子电流平均值逐渐减小;随脉冲频率的增加基体离子电流平均值逐渐减小后趋于稳定;当脉冲宽度为150μs时的基体离子电流平均值高于脉冲宽度为200μs时的基体离子电流平均值。工作参数对膜层的制备具有调制作用, 在适中的工作参数下, 电场增强HiPIMS获得的钒膜与基底结合良好、膜层致密完整。

     

    Abstract: Herein, we addressed the optimization of film growth conditions of the field enhanced high power impulse magnetron sputtering (HiPIMS) reactor.The influence of the deposition conditions, including but not limited to the pressure, target-substrate distance and pulse width/frequency, on the substrate ion current was investigated with scanning electron microscope and oscilloscope.The results show that the growth conditions all have a major impact.For example, the average substrate ion current changed in an increase-leveloff manner with an increase of the pressure at a fixed target voltage, but decreased with an increase of the target-substrate distance; as the pulse frequency increased, it varied in a decrease-constant mode; the average ion current at a pulse-width of 150 μs was higher than that at 200 μs.The dense, compact vanadium coatings with fairly strong interfacial adhesion were grown by field-enhanced HiPIMS under the moderate synthesis conditions.

     

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