Citation: | RONG Zhenhua, CHENG Yongjun, CHEN Lian, SUN Wenjun, DONG Meng, ZHOU Chao, FENG Tianyou, MA Zhanji. A Design of Sorption Characteristics Test Device with Two Test Stations[J]. CHINESE JOURNAL OF VACUUM SCIENCE AND TECHNOLOGY, 2024, 44(3): 243-251. DOI: 10.13922/j.cnki.cjvst.202310007 |
A test device is designed to measure the NEG properties by either the constant pressure or the constant volume method. The device has two test stations with symmetrical structures, which can pretest and test two samples at the same time. The device has a reasonable structure and high test efficiency. The test device can directly output performance parameters by software, such as sorption rate and sorption quantity. The test results show that the vacuum of the device is high, such as the vacuum of the sample chamber is better than 1×10−7 Pa, the leakage rate is less than 3×10−7 Pa·L/s, the test data of the device is high precision and reliable, such as the sorption rate measurement accuracy is 1 mL/s, the sorption quantity measurement accuracy is 1 Pa·mL.
[1] |
单睿, 齐通通, 黎秉哲, 等. 非蒸散型薄膜吸气剂的研究现状及应用进展[J]. 功能材料, 2018, 49(5): 5049−5055(in Chinese)
Shan R, Qi T T, Li B Z, Guo J, Yuan J. Research status and application progress of non-evaporable film getter[J]. Journal of Functional Materials, 2018, 49(5) 5049−5055
|
[2] |
Benvenuti C, Chiggiato P, Cicoira F, et al. Nonevaporable getter films for ultrahigh vacuum applications[J]. Journal of Vacuum Science Technology,1998,16(1):148−154 doi: 10.1116/1.580963
|
[3] |
郭卫斌, 薛函迎, 柴云川. 吸气剂在行波管中的应用[J]. 真空电子技术,2011(4):7−9(in Chinese) doi: 10.3969/j.issn.1002-8935.2011.04.003
Guo W B, Xue H Y, Chai Y C. Application of getters in traveling wave tubes[J]. Vacuum Electronics,2011(4):7−9 doi: 10.3969/j.issn.1002-8935.2011.04.003
|
[4] |
苏童, 艾永昌, 黄水明, 等. MEMS芯片器件用非蒸散型吸气剂的研究状况[J]. 真空科学与技术学报,2021,41(7):674−682(in Chinese)
Su T, Ai Y C, Huang S M, et al. Research situation of non-evaporable getter films for MEMS[J]. Chinese Journal of Vacuum Science and Technology,2021,41(7):674−682
|
[5] |
李晓刚, 罗志芳. 非蒸散型吸气剂吸气性能测试方法的研究[J]. 真空,2017,54(2):60−63(in Chinese)
Li X G, Luo Z F. Research on property measurement system of non-evaporable getter[J]. Vacuum,2017,54(2):60−63
|
[6] |
GB/T 25497-2010吸气剂气体吸放气性能测试方法[S]
|
[7] |
安徽有研吸气材料有限公司. 一种吸气剂材料性能测试装置: CN202220921628.5[P]. 2022−12−09
|
[8] |
合肥工业大学. 一种基于差压法的吸气剂吸气性能测试集成装置: CN202110566941.1[P]. 2021−08−24
|
[9] |
冯天佑, 陈联, 朱建炳, 等. 锆钒铁吸气剂的研究现状及进展[J]. 真空与低温,2017,23(1):7−12(in Chinese) doi: 10.3969/j.issn.1006-7086.2017.01.002
Feng T Y, Chen L, Zhu J B, et al. Research status and development of ZrVFe getter[J]. Vacuum and Cryogenics,2017,23(1):7−12 doi: 10.3969/j.issn.1006-7086.2017.01.002
|
[10] |
苑鹏, 尉秀英, 秦光荣, 等. 锆基吸气剂吸气性能的研究[J]. 稀有金属,2008,32(5):641−644(in Chinese) doi: 10.3969/j.issn.0258-7076.2008.05.020
Yuan P, Wei X Y, Qin G R, et al. Sorption characteristics of Zr-based getters[J]. Chinese Journal of Rare Metals,2008,32(5):641−644 doi: 10.3969/j.issn.0258-7076.2008.05.020
|
[11] |
张艳, 尉秀英, 秦光荣, 等. 钛基非蒸散型吸气剂的性能研究[J]. 稀有金属,2006,30(1):52−55(in Chinese) doi: 10.3969/j.issn.0258-7076.2006.01.012
Zhang Y, Wei X Y, Qin G R, et al. Properties of Ti-based non-evaporable getters[J]. Chinese Journal of Rare Metals,2006,30(1):52−55 doi: 10.3969/j.issn.0258-7076.2006.01.012
|
[12] |
王欲知, 陈旭. 真空技术 [M]. 北京航空航天大学出版社, 2007
|
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